Published September Origi- nally approved in Last previous edition approved in as 3. E – 89a (). Annual Book of ASTM Standards. Buy ASTM E TEST METHODS FOR CHEMICAL ANALYSIS OF COPPER ALLOYS from SAI Global. These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for.
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ASTM E – 03 Standard Test Methods for Chemical Analysis of Copper Alloys
Discard the organic layer. Allow the layers to separate. When dissolution is complete, boil for 1 min to destroy excess peroxide, and cool.
Cool in a desiccator and weigh as nickel dimethylglyoxime. This standard is also available to be included in Asfm Subscriptions. Titrate asstm until the color changes from purplish-red to yellow. Work in a well-ventilated hood. Dilute to mL. The copper oxalyldihydrazide complex is formed with the copper remaining in the electrolyte. Store in a tightly sealed plastic bottle in a dark place. Using indicator paper, check the pH, which should be between 6. The more rapid procedure requires the use of gauze electrodes.
Iron by the 1,Phenanthroline Photometric Test Method [0.
Spiral anodes should be made from 1. The percent variability for the highest calibration solution should be less than 1. Standards Subsctiption may be the perfect solution. Calibration 1 e47 0. If the entire electrolyte is to be used, proceed directly with the neutralization. FORMAT Single User Subscription Site License Subscription BOOKS All Books PACKAGES All Packages EDITION to PUBLISHER. The zinc is then stripped from the organic phase as the ammonia complex, which is further treated with potassium cyanide to complex bivalent metals as well as the zinc.
Allow the layers to separate; then draw off the lower s478 layer into a second separatory funnel.
Standards Subscriptions from ANSI provides a money-saving, multi-user solution for accessing standards. The stem should be made from a platinum alloy wire such as asgm, platinum-rhodium, or platinum-ruthenium, having a diameter of approximately 1.
If no precipitate forms, proceed as directed in Search book title Enter keywords for book title search. Add 8 mL of the DDC solution for each 0. Enter your personal account email address to request a password reset: Store the solution in a polyethylene bottle.
Cast bronze NIST 52c, 0. Register for a trial account. Las Lastt pre previo vious us edi editio tionn ap appro prove vedd in 19 96 as E — 89a Heat until dissolution is complete and then boil the solution for 2 to 3 min. Dilute to volume and mix. Avoid inhalation of e78 and exposure of the skin to the chemical and its solutions. When used in analyses where both cathodic and anodic plates are to be determined, the anodes should be of wire gauze.
If dissolution is difficult, add 0.
Standard Test Methods for Chemical Analysis of Copper Alloys
Using the test cell, take photometric readings of the calibration solutions. Add 50 mL of hot water and, if the solution is clear, proceed as described in Absorbance values are to be used in this calculation. Stir the mixture vigorously and allow to cool to room temperature while stirring occasionally. If they are not, disregard the data, readjust the instrument, and proceed again as directed in Precipitate the iron and tin as before and heat to boiling to coagulate the precipitate.
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Land Use and Development. Quickly remove the cathode, rinse it in water, and then dip into two successive baths of ethanol or methanol. Need more than one copy? A superscript epsilon e indicates an editorial change since the last revision or reapproval.