Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A
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The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the pracitce of reducing carbon content to resist intergranular attack. Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required.
For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions.
Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture d 15 hours. Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals. This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively.
A recent publication on intergranular corrosion. Link to Active This link will always route to the current Active version of the standard. This method is a hour boiling test for “as received” specimens of stainless steel. Work Item s – proposed revisions of this standard. Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself.
Contact us now for pricing or a quote! Referenced Documents purchase separately The documents listed below are referenced within the subject standard but practics not provided as part of the standard. Practice F, is a hour weight-loss based analysis that provides a quantitative aetm of the materials performance, and is commonly used to analyze as-received stainless steels.
Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility. It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries.
Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
ASTM A Intergranular Corrosion Testing and Analysis
In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away. How do you select the right ASTM corrosion testing method for your material?
These practices include five intergranular corrosion tests, namely: Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization.
The Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either “Acceptable” or “Suspect”. Please refer to the specification for more details.
The inch-pound equivalents are in parentheses and may be approximate. At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type. The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:. However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur.
It depends on which Practice is selected, but typically ranges from to days for different tests. In everyday applications, corrosion varies by materials and solutions. What is your typical turnaround time? Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid.
The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice. In many cases we can reduce that to as little as 24 hours more than the required testing time if you need fast results.
Please share this page: For example, many low-carbon and stabilized stainless steels e. Practice B, also known as the Streicher test, uses weight loss analysis to provide a quantitative measure of the materials performance.
The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes.
A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens. Practiec understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur.
Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic pracitce using state-of-the-art equipment. ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
Intergranular corrosion shows up as the dark black lines around the grain boundaries. The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades.
See Appendix X1 for information regarding test selection. The test is generally performed for acceptance of materials, but not sufficient for rejection of materials.
Learn more about our laboratories – where they are located; the unique capabilities they have and how they can help you solve your technical and commercial challenges. Share on Tumblr Print. All five methods within this specification involve exposing specimens to a chemical mixture designed to encourage corrosive behavior.