ASTM a Test, Intergranular Corrosion, IGC, ASTM A Practice, Testing, India – Download as PDF File .pdf), Text File .txt) or read online. ASTM A Practice A test (Oxalic acid test). The oxalic acid etch test is rapid and nondestructive, but not quantitative. It is a rapid etching procedure and . Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.
|Published (Last):||5 February 2018|
|PDF File Size:||15.89 Mb|
|ePub File Size:||18.11 Mb|
|Price:||Free* [*Free Regsitration Required]|
The practicee are etched after metallographic preparation for cross-sectional examination which is thoroughly viewed with a traverse from inside to outside diameters of rods and tubes, from face to face on plates, and across all zones such as weld metal, weld-affected zones, and base plates on specimens containing welds. This method is preferable for chromium depletions and corrosion in intermetallic phases.
This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means.
Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility. The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.
Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels. For example, many low-carbon and stabilized stainless steels e. Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance.
Learn more about our laboratories – praxtice they are located; the unique capabilities they have and how they can help you solve your technical and commercial challenges. These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared.
This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required. It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries.
Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on.
The inch-pound equivalents are in parentheses and may be approximate. Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack.
If the structure is acceptable no additional testing is required. A different ASTM A test method must be used to quantify the level of corrosion or to disqualify a material for use.
Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger pracice intergranular corrosion occurring in use.
ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results.
Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries. Rockwell or Superficial Hardness. Work Item s – proposed revisions of this standard.
Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.
Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard.
Classification of structure then provides either acceptance or further testing required, which typically moves you to one of the next practices. Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation. In everyday applications, corrosion varies by materials and solutions. The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.
Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack. Intergranular corrosion is the proper use, though the specification calls it attack, corrosion is what is taking place.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
It depends on which Practice is selected, but typically ranges from to days for different tests. These tests do not provide a basis for predicting resistance to forms of corrosion other than intergranular, such as general corrosion, pitting, or stress-corrosion cracking. Intergranular simply means that the corrosion is taking place between the grains or crystals, which is where sigma phase or chromium carbides are going to form which makes the material susceptible to IGA.
Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility. The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion.
Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur.
Intergranular Corrosion Testing: An Overview of ASTM A262
Contact us now for pricing or a quote! All austenitic stainless steels should meet this requirement, if proper annealing took place. Because it can be run quickly for screening, we often run this test first.